Preparation of high-density iron soft magnetic materials by HVC technology
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摘要: 以退火純鐵粉末為原料,采用粉末退火結合高速壓制技術的方法制得高密度壓坯(7.70 g·cm-3),經燒結后獲得高密度高性能的純鐵軟磁材料.研究退火粉末的高速壓制行為,以及燒結時間和燒結溫度對材料磁性能和晶粒大小的影響.結果顯示:退火粉末的壓坯密度隨壓制速度的增加而增加,壓坯密度最高可達到7.70 g·cm-3,相對密度可達到98.10%.燒結溫度為1450℃,燒結時間為4 h時,材料密度達到7.85 g·cm-3,相對密度為99.96%,最大磁導率達到13.60 m H·m-1,飽和磁感應強度為1.87 T,矯頑力為56.50 A·m-1.Abstract: High density green compacts of annealed iron powder with a density of 7.70 g·cm-3 were prepared by high velocity compaction(HVC) combined with powder annealing. Iron soft magnetic materials with high performance and high density were obtained after sintering. The HVC behavior of the annealed powder was investigated,and the effects of sintering temperature and sintering time on the magnetic properties and grain size of the soft magnetic materials were studied. The results show that the density of the green compacts increases with increasing compaction velocity,and the maximum density is 7.70 g·cm-3(relative density of 98.10%). Specimens sintered at 1450℃ for 4 h have the optimum magnetic properties,with the sinter density of 7.85 g·cm-3(relative density 99.96%),the maximum permeability of 13.60 m H·m-1,the saturation induction of 1.87 T,and the coercive force of 56.50 A·m-1.
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Key words:
- soft magnetic materials /
- pure iron /
- high density /
- high velocity compaction /
- magnetic properties /
- grain growth
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