Creep fracture of a nickel base single crystal superalloy along [011] orientation
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摘要: 研究了[011]取向的鎳基單晶高溫合金在750~980℃溫度范圍和200~680 MPa應力下的蠕變斷裂特征.在掃描電鏡上對各種實驗狀態下的蠕變斷口和縱向剖面進行了詳細觀察.研究發現:在低溫750℃和中溫870℃不同初始蠕變應力條件下,枝晶間區亞晶界處不規則γ'/γ界面是裂紋主要萌生場所,這些已萌生的裂紋在與外加應力軸垂直的(011)面上沿〈110〉和〈100〉兩個方向擴展;980℃不同初始應力條件下,裂紋主要在合金中顯微疏松孔洞處萌生,沿與外應力軸垂直的方向擴展.觀察750℃和870℃不同應力狀態蠕變試樣的縱向剖面,對亞晶界區不規則γ'相面積分數的測量和計算表明,用面積分數表征該合金[011]取向在中低溫狀態下的蠕變損傷程度是可行的.Abstract: The creep fracture behavior of a[011] oriented single crystal nickel base superalloy was investigated in the temperature range of 750 to 980℃ and the stress scope of 200 to 680 MPa. The fracture surfaces and longitudinal sections of crept specimens were examined by scanning electron microscopy(SEM). It is found that under different initial stresses at 750℃ and 870℃,creep cracks seem always to initiate at the γ'/γ interface on the interdendritic sub-boundary and propagate along the sub-boundary trace,and their cleavage planes expand along〈110〉and〈100〉on the(011) plane. But under different stresses at 980℃,creep cracks initiate at inherent casting pores and slowly propagate perpendicular to the axis of stress applied up to the final fast fracture. After observing the longitudinal sections of specimens crept under different stresses at 750℃ and 870℃,it is feasible for the area fraction of irregularγ' phase in the sub-boundary to characterize the creep damage level before collapsing of the superalloy along the[011]direction at the moderated and low temperatures.
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Key words:
- nickel base superalloys /
- single crystals /
- creep fracture /
- morphology
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