Deformation behaviors during hot compression of GH4700 alloy for 700℃ ultra-supercritical boilers
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摘要: 利用變形溫度為1120~1210℃、應變速率為0.1~20 s-1以及變形量為15%~60%的等溫熱壓縮實驗研究了GH4700合金的熱變形行為.通過對低溫和高應變速率條件下的形變熱效應進行修正,得到準確的流變曲線,推導出描述峰值應力與溫度和應變速率等變形參數的本構方程,并得到GH4700合金熱變形表觀激活能為322 kJ.組織分析表明,動態再結晶是熱變形過程中最主要的軟化方式,再結晶形核方式為應變誘發晶界遷移,變形溫度升高和應變速率增大均有利于再結晶形核.再結晶發展階段,隨著變形量的增大和變形溫度的升高,動態再結晶比例增加,在應變速率-溫度坐標中,再結晶比例等值線呈反"C"形式.采用分段函數描述了不同應變速率下GH4700合金動態再結晶晶粒尺寸與變形參數的關系.Abstract: The hot deformation behavior of nickel-based superalloy GH4700 was investigated by isothermal compression tests at temperatures of 1120 to 1210℃ and strain rates of 0.1 to 20 s-1 with deformations of 15% to 60%. The flow curves at high strain rate and low temperature were corrected in consideration of the deformation-heating effect. Accurate constitutive equations were established between peak stress and deformation parameters, i.e., temperature and strain rate. The activation energy of the alloy was determined to be 322 kJ. Microstructure analysis results show that dynamic recrystallization (DRX) is the principal softening mechanism during hot working. Strain-induced-grain-boundary-migration is the nucleation mechanism, which is promoted by the increase of both temperature and strain rate. The ratio of DRX grains is increased by temperature and strain, while the iso-ratio contour of DRX exhibits an "anti-C" type in the strain rate-temperature coordinate system. The relationship between DRX grain size and deformation parameters was calculated to be a piecewise function which depends on strain rate.
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Key words:
- nickel alloys /
- hot compression /
- dynamic recrystallization /
- deformation heating
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