Microstructural evolution of BFe10-1-1 alloy tubes with continuous columnar grains during dieless drawing
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摘要: 在拉拔速度O.6-0.9mm·s-1、變形溫度750-900℃條件下,對具有連續柱狀晶組織的BFe10-1-1合金管材進行了無模拉拔成形,研究了變形后的微觀組織,探討了其組織演變規律及機理.在本文工藝參數范圍內,晶界平直的連續柱狀晶組織BFe10-1-1合金管材在無模拉拔成形后微觀組織演變為鋸齒形晶界的連續柱狀晶組織.隨拉拔速度和變形溫度的增加,鋸齒的齒深不斷加大.位錯易在接近晶界的區域塞積并躍出晶界,導致在晶界處出現滑移臺階,形成鋸齒形晶界;在滑移變形的同時,粗大的連續柱狀晶開始轉動,加劇了鋸齒化的程度.高的熱激活能和變形儲存能未能及時釋放是BFe10-1-1合金保持連續柱狀晶組織的根本原因.Abstract: The dieless drawing forming of BFel0-1-1 alloy tubes with continuous columnar grains was performed in a temperature range of 750-900℃ at a drawing speed of 0.6-0.9 mm·s-1. The mierostructural evolution and mechanism of the tubes after the deformation was studied by optical microscopy, transmission electron microscopy, and X-ray diffraction analysis. It is found that the straight grain boundaries of colmnnar grains in the tubes become zigzag after dieless drawing within the process parameters of this paper. The sawtooth depth increases both with increasing drawing speed and temperature. Dislocations tend to pile up adjacent to grain boundaries and then travel over the grain boundaries, leading to gliding steps at the grain boundaries and consequently zigzag grain boundaries. Accompanied with the gliding deformation, thick continuous columnar grains start to rotate, increasing the zigzag degree. The high thermal activation energy and deformation-stored energy failed to release in time are the cause of maintaining continuous columnar grains in BFe10-1-1 alloy.
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Key words:
- copper alloys /
- dieless drawing /
- columnar grains /
- microstructural evolution /
- grain boundaries
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