Microstructural evolution in quenching & partitioning steel during partitioni process
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摘要: 利用掃描電鏡、透射電鏡、X射線衍射和電子探針等研究了0.2C-1.51Si-1.84Mn鋼在配分階段組織的演變情況.配分溫度為400℃時,碳在10 s時就可以完成配分,得到殘余奧氏體最大體積分數為13.4%.隨著配分時間的增長,鋼中馬氏體發生回火現象,奧氏體發生分解,強度、延伸率降低.當配分時間達到1000 s時,屈服強度、延伸率突然升高.分析認為馬氏體回火帶來的塑性提高抵消了殘余奧氏體量減少引起的塑性降低,并且由于滲碳體和碳化物的析出,變形時阻礙位錯的運動,從而提高了屈服強度.通過電子探針分析說明配分階段發生了碳的擴散,隨著配分時間的增長,發生了滲碳體和碳化物的析出,降低了殘余奧氏體中碳的含量.Abstract: Microstructural evolution in 0.2C-1.51Si-1.84Mn steel during partitioning process was studied by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD) and electron microprobe analysis (EMPA). When partitioning at 400℃, carbon atoms have redistributed within 10 s, and the volume fraction of retained austenite is 13.4%. When the partitioning time increases, martensite is tempered and austenite decomposes, leading to the decrease of strength and elongation. However, when the partitioning time is 1 000 s, the tensile strength and elongation suddenly increase. The reason is that the elongation loss caused by decomposition of retained austenite is offset by tempered martensite, the precipitation of carbides and cementite impedes dislocation movement, and thus its tensile strength increases. EPMA results show that carbon atoms diffuse during partitioning process, and carbides and cementite precipitate when the partitioning time increases, which decreases the content of carbon in retained austenite.
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Key words:
- steel heat treatment /
- microstructural evolution /
- austenite /
- martensite /
- electron probe analysis
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