Stability of reversed austenite in 9Ni steel
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摘要: 為了研究逆轉變奧氏體在應力和低溫條件下的穩定性,通過透射電子顯微鏡對淬火+回火(QT)和淬火+兩相區淬火+回火(QLT)處理9Ni鋼中逆轉變奧氏體進行形貌觀察.結果發現QT處理鋼中逆轉變奧氏體以塊狀形態存在;QLT處理鋼中逆轉變奧氏體以塊狀和薄膜狀存在,薄膜狀逆轉變奧氏體分布在板條邊界上.通過X射線衍射對液氮浸泡前后逆轉變奧氏體含量和其碳含量的變化進行測量,發現QLT工藝處理后在液氮中穩定存在的逆轉變奧氏體的含量要高于QT工藝.通過三點彎曲試驗、單軸拉伸和壓縮試驗研究其機械穩定性,發現拉應力和壓應力均能促使逆轉變奧氏體轉變,大部分殘留奧氏體分布在晶內.Abstract: To evaluate the stability of reversed austenite under the condition of stress and low temperature, the morphologies of reversed austenite in 9Ni steel after the treatments of quenching + tempering (QT) and quenching + lamellar quenching + tempering (QLT) were observed by transmission electron microscopy. Reversed austenite in the QT-treated sample is most lath-like; but in the QLT-treated sample, both thin foil and lath reversed austenite can be discovered and the former mainly turns up along lath martensite. The amount of reversed austenite and its carbon content before and after soaking in liquefied nitrogen were measured by X-ray diffraction. More stable reversed austenite is detected in the QLT-treated sample after soaking in liquefied nitrogen. The mechanical stability of reversed austenite was gauged by bending, uniaxial tensile and compression tests. Both the tensile and compress stress promote the reversed austenite to transform, and most of residual austenite are revealed within grains.
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Key words:
- alloy steel /
- austenite /
- thermal stability /
- mechanical stability /
- cryogenic equipment
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