氟化物熔體中電解共沉積硼化鈦的陰極過程

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氟化物熔體中電解共沉積硼化鈦的陰極過程

段淑貞, 石青榮, 王新東, 苑聯雨

文章導航 > 工程科學學報 > 1996 > 18(1): 46-49

段淑貞, 石青榮, 王新東, 苑聯雨. 氟化物熔體中電解共沉積硼化鈦的陰極過程[J]. 工程科學學報, 1996, 18(1): 46-49. doi: 10.13374/j.issn1001-053x.1996.01.011

引用本文:

段淑貞, 石青榮, 王新東, 苑聯雨. 氟化物熔體中電解共沉積硼化鈦的陰極過程[J]. 工程科學學報, 1996, 18(1): 46-49. doi: 10.13374/j.issn1001-053x.1996.01.011

Duan Shuzhen, Shi Qingrong, Wang Xindong, Yuan Lianyu. Cathode Process in the Electrolytic Codeposition of Titanium Diboride in Molten Fluoride[J]. Chinese Journal of Engineering, 1996, 18(1): 46-49. doi: 10.13374/j.issn1001-053x.1996.01.011

Citation:

Duan Shuzhen, Shi Qingrong, Wang Xindong, Yuan Lianyu. Cathode Process in the Electrolytic Codeposition of Titanium Diboride in Molten Fluoride[J]. Chinese Journal of Engineering, 1996, 18(1): 46-49. doi: 10.13374/j.issn1001-053x.1996.01.011

段淑貞, 石青榮, 王新東, 苑聯雨. 氟化物熔體中電解共沉積硼化鈦的陰極過程[J]. 工程科學學報, 1996, 18(1): 46-49. doi: 10.13374/j.issn1001-053x.1996.01.011

引用本文:

段淑貞, 石青榮, 王新東, 苑聯雨. 氟化物熔體中電解共沉積硼化鈦的陰極過程[J]. 工程科學學報, 1996, 18(1): 46-49. doi: 10.13374/j.issn1001-053x.1996.01.011

Duan Shuzhen, Shi Qingrong, Wang Xindong, Yuan Lianyu. Cathode Process in the Electrolytic Codeposition of Titanium Diboride in Molten Fluoride[J]. Chinese Journal of Engineering, 1996, 18(1): 46-49. doi: 10.13374/j.issn1001-053x.1996.01.011

Citation:

Duan Shuzhen, Shi Qingrong, Wang Xindong, Yuan Lianyu. Cathode Process in the Electrolytic Codeposition of Titanium Diboride in Molten Fluoride[J]. Chinese Journal of Engineering, 1996, 18(1): 46-49. doi: 10.13374/j.issn1001-053x.1996.01.011

氟化物熔體中電解共沉積硼化鈦的陰極過程

doi: 10.13374/j.issn1001-053x.1996.01.011

北京科技大學物理化學系, 北京 100083

基金項目:

國家自然科學基金,金屬腐蝕與防護國家重點實驗室資助

作者簡介:
段淑貞女 65歲教授

中圖分類號: TF123.132;TF123.32
計量
- 文章訪問數: 182
- HTML全文瀏覽量: 57
- PDF下載量: 5
- 被引次數: 0
出版歷程
- 收稿日期: 1995-08-19
- 網絡出版日期: 2021-10-29

Cathode Process in the Electrolytic Codeposition of Titanium Diboride in Molten Fluoride

Department of Physical Chemistry, USTB, Beijing 100083, PRC

摘要: 采用循環伏安法首次研究了LiF-NaF-K₂TiF₆-KBF₄熔鹽體系中鈦離子和硼離子在鉑、鉬電極上電化學還原及電合成硼化鈦的陰極過程機理。對恒電位電解的沉積物進行了X射線衍射分析。結果表明,當體系中硼鈦摩爾比B/Ti大于2時,鈦與硼可在同一電位下實現電解共沉積并反應生成硼化鈦。
- 硼化鈦 /
- 電解共沉積 /
- 電合成 /
- 氟化物熔鹽
Abstract: The mechanism of the electrochemical reduction of Ti(Ⅳ) and B(Ⅲ) as well as the electrochemical synthesis of TiB₂ on platinum and molybdenum electrode in molten Li-NaF-K₂TiF₆-KBF₄ system has been investigated for the first time by. Means of cyclic voltammetry. The electrodeposited coating has been analysed by X-ray diffraction. The results show that the electrolytic codeposition of titanium and boron with the formation of TiB₂ can be achieved at molar ratios B/Ti>2.
- titanium diboride /
- electrolytic codeposition /
- electrochemical synthesis /
- molten fluorides

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文章訪問數: 182
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PDF下載量: 5
被引次數: 0

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