High Temperature Low Cycle Fatigue of GH133 Superalloy
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摘要: 本文研究了GH133合金的循環應力應變反應和低周疲勞性能,并作了位錯結構和斷口觀察。通過對比拉壓對稱(R=-1)試驗和恒定最大正應變(εmax=C)試驗,證明平均拉應力起降低壽命的作用。位錯結構觀察證明,循環使共格γ′質點的相界處產生應力場,最終導致位錯的萌生并運動,位錯運動又進一步增殖位錯。位錯運動方式是變化的,由成對切割γ′質點到單位錯切割γ′質點和位錯繞過γ′質點。滑移帶位錯結構最終可以出現飽和的梯狀結構,與典型的駐留帶位錯結構相似。晶界和雙晶界附近位錯密度高,具有位錯胞結構,同時可以出現沿晶界裂紋和沿雙晶界裂紋。
在循環交變作用下,材料的破壞過程可以分解為三個主要過程,即在循環作用下產生的材料變形行為的變化,疲勞裂紋的形成和疲勞裂紋不斷擴展,直到一定的臨界大小而發生最終破壞,這三個過程是不同的但又是相互聯系的,宏觀疲勞現象可以在此基礎上作出適當的說明。對于含有共格γ′沉淀相的低層錯能奧氏體合金,許多研究[1—8]指出,其循環反應往往是先循環硬化再循環軟化,并具有面排列位錯結構。關于循環軟化現象,一些作者認為[8],共格沉淀相在位錯往復切割下碎化而導致回溶,...Abstract: The cyclic stress-strain responce and microstructures(TEM) were studied in LCF samples of 15Cr-27Ni-1.8Ti-Fe alloy. The strain control LCF tests were performed at 600* under two different wave mode:R=-1 and fixed eeeemax. Comparing the results of these two kind tests, the detrimantal effect of average tensile stress was proved. This was comcerned with the influenceof tensile stress on the movement of dislocations and the fromation ocracks.
The observations of dislocations structure indicated that during the cycling both mechanisms causing cyclic hardening and cyclic softening were taking place. Cyclic strain led to generate the stress-field at the interface of γ and γ' phases first. As a result of increasing stress field the dislocations were created.The density of dislocation was further increased by the move, ment of dislocations themself. The interactions between dislocations and γ particles degenerated from pair dislocation cutting γ' particles to single dislocation cutting γ'particles. It led to form more faults and APB'S, and the γ' particles became propressively harder to shear and ultimately led to dislocations looping around particles.
A typical dislocation structure of persistant slip hand, laddie-like stracture was seen asasatureted dislocation structure in the slip band,and the more laddie-like structure formed, the more cyclic softening happened.
The slip band extended to grain boundaries and twin boundaries, The grain diclocations interacted with boundaries, and led to complex boundary dislocations structure the density of dislocations near grain boundaries andtwin boundaries was much higher than others since the boundaries can actedas the barrier and dislocation generator. This would cause to form grainboundary cracks and twin boundary cracks. -

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