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基于微型塌落筒實驗的充填料漿屈服應力表征

Characterization of filling slurry yield stress based on a mini-slump cone test

  • 摘要: 充填料漿的管道輸送是充填采礦法的一個重要環節,而充填料漿的流變參數是評價充填料漿管輸特性的重要指標,目前主要采用流變儀進行測定,但礦山現場通常不具備流變實驗條件,主要通過塌落度實驗來評價充填料漿的流動性能。本文采用微型塌落筒進行不同質量分數、灰砂比的充填料漿塌落度實驗,建立微型塌落筒擴展度與屈服應力之間的解析模型,根據料漿停止流動后的形態得到簡化計算模型,基于簡化模型理論計算料漿的屈服應力,并將理論值與流變儀測試同等配比條件下得到的屈服應力實驗值進行對比分析,同時通過雙因素方差分析研究了不同質量分數、灰砂比對充填料漿擴展度的影響規律。結果表明,擴展度主要受質量分數的影響,灰砂比對其影響不顯著,充填料漿的屈服應力隨質量分數的增大而增大。在質量分數較低時,理論值與實驗值的相對誤差范圍較大,二者的相對誤差在25%以內,平均誤差為16.79%;隨著質量分數增大,誤差逐漸減小至15%以內,平均誤差為8.81%。綜合考慮質量分數的影響,提出基于質量分數的修正系數,修正后的屈服應力理論值與實驗值的相對誤差降至10%以內,平均誤差為3.54%。本研究微型塌落筒實驗較傳統塌落度實驗不僅節省實驗用料和勞動強度,還可有效表征料漿屈服應力,對于礦山充填料的流動性能評價具有實際指導意義。

     

    Abstract: The backfill mining method is widely used in mines because of its advantages of environmental protection, safety, and efficiency and includes filling slurry pipeline transportation as an important part. The rheological parameters of filling slurry are important indicators for evaluating the characteristics of filling slurry pipeline transport; these parameters are mainly determined by rheometers at present, while the rheological experimental conditions are usually unavailable at the mine site. Because of its simplicity and speed, mines mainly use a slump test to evaluate the flow properties of a filling slurry. In this paper, we used a mini-slump cone to conduct a slump experiment of filling slurry with different mass fractions and cement–tailings ratios (the two most common variable parameters in filling slurry ratios), established an analytical model between the spread of a mini-slump cone and yield stress, obtained a simplified calculation model according to the shape of the filling slurry after flowing, calculated the yield stress of the slurry based on the simplified model, and compared the theoretical value with the experimental value of the yield stress of the filling slurry under the condition of the same ratio tested by a rheometer. At the same time, the influence law of different mass fractions and cement–sand ratios on the expansion degree of the filling slurry was studied using a two-factor analysis of variance. The results show that the spread is mainly influenced by the mass fraction and unsubstantially affected by the cement–sand ratio. The yield stress of the filling slurry increases with the mass fraction. When the mass fraction is low, the error in the theoretical value relative to the experimental value has a large range, and the error in the theoretical value is within 25%, averaging 16.79%; as the mass fraction increases, this error gradually decreases below 15%, averaging 8.81%. Considering its effect, a correction factor based on the mass fraction was proposed, and the error in the theoretical yield stress value after the correction was reduced below 10%, averaging 3.54%. In this study, the mini-slump cone test not only reduces the experimental material and labor intensity compared with the traditional slump test but also effectively characterizes the yield stress of the slurry, which provides practical guidance for evaluating the flowability of mine filling slurry.

     

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