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兩相區位錯增殖對低碳貝氏體/鐵素體復相鋼組織和性能的影響

Effect of dislocation multiplication in intercritical region on microstructure and properties of low-carbon bainite/ferrite multiphase steel

  • 摘要: 利用掃描電子顯微鏡(SEM)、透射電子顯微鏡(TEM)、電子探針(EPMA)、X射線衍射儀(XRD)、室溫拉伸等手段, 通過兩相區保溫-淬火(IQ)、兩相區形變后保溫-淬火(DIQ)、兩相區保溫-淬火-配分-貝氏體區等溫(IQ&PB)及兩相區形變后保溫-淬火-配分-貝氏體區等溫(DIQ&PB)熱處理工藝, 研究高溫形變對室溫組織、性能、殘余奧氏體穩定性的綜合影響作用.結果表明, 經15%的壓縮形變后鐵素體中位錯密度由0.290×1014增加至1.286×1014 m-2, 馬氏體(原奧氏體)中C、Cu元素富集濃度提高, 高溫形變產生位錯增殖對元素配分有明顯促進作用.DIQ&PB工藝下, 形變后貝氏體板條尺寸變短且寬度增加0.1 μm左右, 貝氏體轉變量較未變形時增加14%, 多邊形鐵素體尺寸明顯減小.力學性能方面, 兩相區形變熱處理后抗拉強度增加132.85 MPa, 斷后伸長率增加7%, 強塑積可達25435 MPa·%.形變后殘余奧氏體體積分數由7.8%提高到8.99%, 殘余奧氏體中碳質量分數由1.05%提高到1.31%.

     

    Abstract: Hot deformation is a way to effectively improve strength and plasticity of multiphase steels simultaneously, thereby, improving mechanical properties of multiphase steels. Hot deformation affects martensitic transformation mechanism, microstructure, and mechanical properties because it increases retained austenite content and improves stability of multiphase steels. Moreover, hot deformation plays a role in dislocation multiplication, and fine grain strengthening; it can reduce bainite transformation driving force, reduce bainite transformation point, and result in small multiphase organization after quenching-partitioning process. The result can significantly improve the properties of materials. The effects of high-temperature deformation on the stability of room-temperature microstructure, mechanical property, and retained austenite under treatment of IQ&PB (intercritical annealing-quenching and partitioning within the bainitic region) and DIQ&PB (intercritical deformation-intercritical annealing-quenching and partitioning within the bainitic region) processes were studied using scanning electron microscopy (SEM), transmission electron microscope (TEM), electron probe X-ray microanalyser (EPMA), X-ray diffraction (XRD), and tensile testing machine. The results show that dislocation density increases from 0.290×1014 to 1.286×1014 m-2 after 15% compression deformation, and the respective concentrations of C and Cu element enrichment in martensite (the original austenite) increases. Overall, dislocation multiplication produced by high-temperature deformation significantly promotes elemental distribution. After the deformation, the size of bainite lath shortenes and its width increases by 0.1 μm, the volume of the bainite transition increased by 14%, and the size of the polygonal ferrite significantly decreases under the DIQ&PB treatment. In terms of mechanical properties, the tensile strength increases by 132.85 MPa, and the elongation increases by 7%; the strength and ductility product reaches 25435 MPa·% after intercritical deformation heat treatment. The volume fraction of retained austenite increases from 7.8% to 8.99%, and the mass fraction of carbon in the retained austenite increases from 1.05% to 1.31% after compression deformation.

     

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