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工藝參數對連續定向凝固Cu-12%Al線材表面質量、組織和性能的影響

Effects of process parameters on the surface quality, microstructure and mechanical properties of Cu-12%Al wires fabricated by continuous unidirectional solidification

  • 摘要: 采用真空熔煉、氬氣保護下拉式連續定向凝固方法制備了直徑為6mm的Cu-12%Al(質量分數)合金線材,并研究了結晶器長度、熔體溫度和拉坯速度對線材表面質量、組織和力學性能的影響.結果表明:在結晶器長度為20~40mm,熔體溫度為1100~1250℃,拉坯速度為10~70mm·min-1范圍內,可以穩定制備出具有單晶或柱狀晶組織的線材.縮短結晶器長度、提高熔體溫度或拉坯速度均有利于改善線材表面質量;降低熔體溫度、增加結晶器長度或提高拉坯速度連鑄有利于獲得連續柱狀晶組織.當結晶器長度為30mm,熔體溫度為1100~1150℃,拉坯速度為10~70mm·min-1時,線材橫截面晶粒尺寸隨拉坯速度的增加先減小而后增加.在結晶器長度30mm,熔體溫度1150℃,拉坯速度30mm·min-1條件下制備的連續柱狀晶組織線材,其延伸率可達25.7%.

     

    Abstract: Cu-12%Al alloy wires with a diameter of 6 mm were prepared by vacuum melting and argon shield vertical continuous unidirectional solidification process. The effects of melt temperature, crystallizer length and drawing velocity on the surface quality, microstructure and mechanical properties of the alloy wires were investigated. The results show that single-crystalline or columnar-crystalline wires can be fabricated at a crystallizer length of 20 to 40 mm, a melt temperature of 1100 to 1250℃ and a drawing velocity of 10 to 70 mm·min-1. Shortening the crystallizer length, raising the melt temperature and/or increasing the drawing velocity are in favor of improvements in the surface quality, but the continuous columnar-crystalline wires can be obtained at a lower melt temperature, a longer crystallizer length and/or a higher drawing velocity. With the increase of drawing velocity, the cross-sectional grain size of the wires decreases firstly and then increases in the parameter regions of the crystallizer length of 30 mm, the melt temperature of 1 100 to 1 150℃ and the drawing velocity of 10 to 70 mm·min-1. The continuous columnar-crystalline wires manufactured at the crystallizer length of 30 mm, the melt temperature of 1 150℃ and the drawing velocity of 30 mm·min-1 have a good elongation percentage of 25.7%.

     

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