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粉煤灰基多孔陶瓷過濾材料的制備和性能

Preparation and performance of fly ash porous ceramics for filtration

  • 摘要: 以粉煤灰為骨料,采用添加造孔劑法制備粉煤灰基多孔陶瓷過濾材料,研究了造孔劑用量和燒結溫度對其性能的影響.通過壓汞儀、X射線衍射儀和場發射掃描電子顯微鏡等分析測試技術對試樣進行了性能表征.結果表明:隨著造孔劑用量的增加,顯氣孔率和吸水率升高,抗彎強度和密度下降.提高燒結溫度可以有效提高抗彎強度,而不影響材料的主要物相組成;當燒結溫度大于1175℃時,顯氣孔率和透氣度顯著下降.造孔劑用量為35%,燒結溫度為1175℃時,可制得抗彎強度大、氣孔發達及高比表面積的多孔陶瓷過濾材料.

     

    Abstract: Porous ceramics were prepared from fly ash by adding a pore-making agent. Some effects of the amount of the poremaking agent and sintering temperature on the properties of the porous ceramics were studied. The properties of specimens were characterized by pressure mercury analyzer, X-ray diffraction (XRD), and field emission scanning electron microscopy (SEM). The results show that with the pore-making agent increasing, the porosity and water absorption increase, but the bending strength and density decrease. Increasing the sintering temperature can improve the bending strength of the porous ceramics. However, main phases in the porous ceramics are similar at different sintering temperatures. As the sintering temperature is more than 1175℃, the porosity and gas permeability decrease significantly. When the amount of the pore-making agent is 35% and the sintering temperature is 1175℃, the fly ash porous ceramics for filtration have high bending strength, advanced porosity and high specific surface area.

     

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