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一種001取向鎳基單晶高溫合金蠕變特征

Creep characteristics of a Ni base single crystal superalloy along 001 direction

  • 摘要: 研究了一種001取向鎳基單晶合金的蠕變特征和變形期間的微觀組織結構.結果表明:在低溫高應力和高溫低應力條件下,合金具有較長的蠕變壽命和較低的穩態蠕變速率;在700℃,720MPa條件下,透射電鏡(TEM)觀察顯示蠕變期間的變形特征是\frac12<110>位錯在基體中運動,發生反應形成\frac13<112>超肖克利(Shockley)不全位錯,切入γ'相后產生層錯.在900℃,450MPa條件下,沒有出現蠕變初始階段,γ'相從立方體形態演化成筏形;在加速蠕變階段,多系滑移開動,大量位錯剪切γ'相是變形的主要機制.在1070℃,150MPa條件下,γ'相逐漸轉變成筏形組織,并在γ/γ'界面處形成致密的六邊形位錯網,位錯網可以阻止位錯切入γ'相,提高蠕變抗力;在蠕變后期,位錯以位錯對形式切入γ'相,是合金變形的主要方式.

     

    Abstract: An investigation was conducted on the creep behavior and microstructure of a Ni base single crystal superalloy with 001 orientation during creep deformation.The results show that the test samples exhibited a lower steady creep rate and a longer creep life under the higher temperature and stress level.Under the condition of 700℃ and 720MPa TEM observations indicate that \frac12<110> dislocations move in the matrix and react to form the Shockley segments of \frac13<112> dislocations,which cut into the γ' phase and form stacking faults in the precipitates.Under the condition of 900 ℃ and 450MPa,the primary creep stage does not appear.The morphological evaluation of the γ' phase develops from original cubic to raft microstructure.Multiple slip operates and dislocations shearing the γ' phase is the main deformation mechanism during the creep acceleration stage.Under the condition of 1070 ℃ and 150MPa,it is found that the γ' phase gradually changes into raft microstructure,hexagonal dislocation networks appear on the γ/γ' interface,and the regular and dense dislocation networks can inhibit dislocations cutting into the γ' phase and enhance the creep resistance.In the later creep stage,the main deformation characteristic is that the γ' phase is sheared by dislocation pairs.

     

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