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超細赤鐵礦粉非熔態還原實驗研究

Experimental study on reduction of ultra-fine hematite powder at non-molten state

  • 摘要: 研究了平均粒度為2μm的超細赤鐵礦粉和粒度分布為0.18~0.154mm的常規細礦粉在非熔態下的還原情況.以礦粉的還原度為目標,用改造后的L16(215)正交表安排4×23次試驗,以排除還原氣氛、還原溫度和還原時間等因素的干擾.結果表明,在純H2、100%CO兩種氣氛下,溫度為650~850℃時,均能實現不同程度Fe2O3→Fe的還原,與常規粒度礦粉相比,超細礦粉的還原度較高,獲得相同還原度時所需的還原溫度約低365℃.試驗中,各因子之間均無相關性,可分別估計其定量的影響,建立線性回歸式.超細赤鐵礦粉非熔態還原后的粒度分布觀察表明,顆粒間并未發生燒結,還原產物仍為粉狀.

     

    Abstract: The reduction degrees of ultra-fine hematite powder(the average particle size is 2μm) and conventional hematite powder(the range of particle size is 0.18 to 0.154mm) in non-molten process were studied.Taking the reduction degree of hematite powder as a target and according to the transformed L16(215) orthogonal table,a series of 4×23 times experiments were arranged to eliminate the interference of reduction atmosphere,reduction temperature and reduction time.The results show that ultra-fine hematite powder can be reduced from Fe2O3 to Fe at different degrees.Compared with conventional particle size hematite powder,ultra-fine hematite powder has a higher reduction degree,and the reduction temperature required to access the same reduction degree lowers about 365 ℃ under the condition of 650 to 850 ℃ and pure H2 or 100% CO atmosphere.There is no correlation among these factors,the quantitative impact of them can be separately estimated,and this provides a basis for establishing an equation of linear regression for each of them.After reduction at non-molten state,the particle size distribution of hematite powder indicates that inter-particle sintering does not occur and the reduction product is still powdery.

     

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