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超音速氣霧化制備316L不銹鋼粉末的表征

Characterization of 316 L stainless steel powders produced by supersonic gas atomization

  • 摘要: 利用自行研制的超音速霧化技術制備了316L不銹鋼粉末,采用激光粒度儀、掃描電鏡、金相顯微鏡和X射線衍射儀進行了表征.結果表明,316L不銹鋼粉末的平均粒度約為24μm,粒度分布的幾何標準偏差δ為1.75;粉末內部存在三種典型凝固組織,即具有發達二次枝晶的枝晶組織、胞晶組織以及枝狀晶與胞狀晶的混合組織;大粒徑氣霧化316L不銹鋼粉末為單一的γ奧氏體相,小粒徑粉末由γ奧氏體相+少量δ鐵素體相共同組成;熔滴的冷速隨著粒徑的減小而提高,平均冷卻速率為104~107K·s-1.

     

    Abstract: 316 L stainless steel powders were prepared by supersonic gas atomization.The characteristic of the powder particles was investigated by means of laser particle size analyzer,scanning electron microscopy(SEM),optical microscopy(OM) and X-ray diffraction(XRD) technique.The result indicates that the mass median particle diameter is about 24 μm and the geometric standard deviation δ is 1.75.Three main types of solidification microstructures were observed in the powders:well-developed dendrite,cellular and a mixture of dendrite and cellular.XRD measurements show that γ-austenite phase is found in the big particle while small particle is a composite consisting of δ-ferrite and γ-austenite phases.The cooling rate is inversely related to the particle size,i.e.,it increases with decreasing particle size.The mean cooling rates of melt droplets range from 104 to 107 K·s-1.

     

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