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碳化硅陶瓷的放電等離子燒結

Spark olasma sintering of silicon carbide

  • 摘要: 采用添加了Al2O3和Y2O3助燒劑的碳化硅微粉為原料,通過放電等離子燒結(SPS)技術快速制備了碳化硅陶瓷.分析了材料致密化過程,并重點研究了燒結工藝參數對材料致密度和力學性能的影響規律.結果表明,當SPS工藝參數的燒結溫度和壓力分別為1600℃和50MPa時,經過5min的燒結,碳化硅陶瓷的致密度可達到99.1%,硬度為HV2550,斷裂韌性達8.34MPa·m1/2,彎曲強度達684MPa.

     

    Abstract: Silicon carbide (SIC) ceramics with submicron silicon carbide as raw material and Al2O3 and Y2O3 as sintering additives were fabricated by spark plasma sintering (SPS). The densification process of the materials was analyzed, and the effects of sintering temperature, sintering pressure and time on the densification and mechanical properties were investigated. It is found that the SiC with a relative density of 99.1% can be achieved when the sintering temperature, sintering pressure and holding time are 1 600℃, 50 MPa and 5 min, respectively. The mechanical properties of the sintered SiC are HV 2550 in hardness, 8.34 MPa·m1/2 in fracture toughness and 684 MPa in bending strength.

     

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