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注射成形0Cr17Mn11Mo3N無鎳高氮不銹鋼的燒結

Sintering of nickel-free high nitrogen 0Cr17MnllMo3N stainless steel prepared by powder injection molding

  • 摘要: 采用粉末注射成形技術制備了0Cr17Mn11Mo3N無鎳高氮奧氏體不銹鋼,研究了各燒結工藝參數(溫度、時間、氣氛)對其相對密度及氮含量的影響.結果表明:溫度是最重要的燒結參數,提高溫度可以顯著增加燒結體的相對密度,但引起氮含量的下降,在1300℃以上燒結,燒結體相對密度可達99%以上;燒結時間所起作用不明顯,燒結2 h足夠使粉末致密化過程完成;氣氛對0Cr17Mn11Mo3N不銹鋼的燒結影響顯著,在N2+H2混合氣中燒結比在純N2氣中獲得更高的相對密度及更低的氮含量.0Cr17Mn11Mo3N不銹鋼的最佳燒結條件為:溫度1300℃,時間2 h,氣氛采用流動的高純氮氣,此時燒結體相對密度達到99.1%,氮質量分數為0.78%.

     

    Abstract: A kind of nickel-free high nitrogen austenitic stainless steel (0Cr17Mn11Mo3N) was prepared by powder injection molding. The effects of sintering parameters such as temperature, time and atmosphere on the relative density and nitrogen content were investigated. The results show that sintering temperature is the most important sintering parameter, with the increase of which the relative density of sintered specimens increases remarkably, whereas the nitrogen content decreases, and above 1 300 E the relative density of sintered specimens is over 99%. Sintering time has no obvious effect on the relative density and nitrogen content, and when the sintering temperature is high enough, the excellent densification of the powder can be achieved within 2 h. For the sintering of 0Cr17Mn11Mo3N stainless steel, sintering atmosphere has also a significant influence, and the higher relative density and lower nitrogen content can be obtained in N2 + H2 atmosphere than in high purity N2 atmosphere. The optimal sintering conditions of 0Crl7MnllMo3N austenitic stainless steel are as follows:1 300℃, 2 h, and flowing high pure nitrogen. Under the optimal conditions, the relative density of sintered specimens can reach 99.1% and the mass fraction of nitrogen is as high as 0.78%.

     

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