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定向凝固過程中的流動效應

Convective effects during unidirectional solidification

  • 摘要: 在類合金(NH4Cl-H2O溶液)定向凝固晶體生長實驗裝置上,利用?30μm煤粉作示蹤粒子,再現糊狀區內微通道流以及通道出口處的流體流動,并測算了各處流體的瞬時速率.分析認為:凝固初期,糊狀區內固相體積分數較大,內部流體流動受阻;隨著固相體積分數減少,糊狀區孔隙率增大,流體充分發展;當平均固相體積分數降至0.42,接近最小值0.38時,當量雷諾數達到臨界值(247),糊狀區內形成微通道;隨著通道寬度逐漸擴大,液相區內熱流體進入微通道.微通道內稀冷液體向上流,濃熱液體向下流,促使通道內溶液再結晶.

     

    Abstract: Directional solidification experiments were carried out using the analogue casting system of NH4Cl-H2O solution by cooling it from below. The transient velocities of fluid flow within the micro-channel of mushy layer were measured by using observation facility and tracer coal particles of 30 μm in diameter. It turned out that during the solidification process, the mean solid fraction of mushy layer descended rapidly at first, so the mushy layer got more permeable and natural convection was more likely to occur. When the mean solid fraction was down to 0.42, and closed to the smallest value of 0.38, and the equivalent Reynolds number exceeded the critical value, about 247, plume convection with associated micro-channel occurred in the mush. With the expanding of channel width, the solution of liquid region, whose temperature was higher than that of mushy layer, flowed into the micro-channel. The convection within the channel was found to consist of upward flow and downward flow. The counter flow advected heat away and solute which was favorable to solidification, so that solution within the channel recrystallized.

     

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