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熱處理溫度對金屬Al增韌氧化鋁多孔陶瓷支撐體斷裂韌性的影響

Effects of heating temperature on the fracture toughness of macroporous alumina supports added Al powder

  • 摘要: 采用干壓成型法,通過添加適量的金屬Al粉來增韌Al2O3多孔支撐體,詳細考察了熱處理溫度對多孔Al2O3/Al支撐體力學性能的影響,并借助于掃描電子顯微鏡(SEM)分析了樣品的微觀結構.研究結果表明:當熱處理溫度較低時,支撐體內部大量未氧化的鋁相是支撐體斷裂韌性提高的主要的原因;當熱處理溫度較高時,鋁氧化產生體積膨脹,膨脹裂紋對支撐體斷裂韌性的提高貢獻很大.

     

    Abstract: An amount of Al powder was added to toughen Al2O3 porous supports by dry press forming. Based on the toughening mechanism of Al2O3/Al composite, the effects of heating temperature on the fracture toughness and bending strength of macroporous Al2O3/Al supports were investigated in detail, and the microstructure of specimens made of the supports was analyzed by SEM. The results show that the fracture toughness of the supports is influenced by calcining temperature. When the calcining temperature is low, unoxidized Al phase can absorb amount of fracture energy to make the fracture toughness of the supports high. But when the temperature is above 1200℃, the cracks which is occurred in the oxidation processing of Al phase can improve the fracture toughness of the supports, and the contribution of cracks is more important than the amount of Al phase to the fracture toughness of supports.

     

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