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注氫誘發ODS鐵素體鋼中第二相分解

Effect of hydrogen ion implantation on the microstructure of ODS ferritic steel

  • 摘要: 采用室溫離子注入和低壓電鏡原位觀察的方法,研究了注氫對國產ODS鐵素體鋼微觀結構的影響.結果表明:原始未注氫ODS鐵素體鋼中存在有一定數量的(Fe,Cr)2O3,室溫注氫后,(Fe,Cr)2O3無明顯改變;但將其加熱至450℃,(Fe,Cr)2O3即開始分解;到550℃時,部分(Fe,Cr)2O3消失,殘余(Fe,Cr)2O3的成分也發生了改變.與此相反,原始未注氫ODS鐵索體鋼的微觀結構在加熱過程中卻沒有明顯改變,(Fe,Cr)2O3并不分解.

     

    Abstract: The effect of hydrogen ion implantation on the microstructure ofODS ferritic steel was studied by means of ion implantation at room temperature and in-situ observations in a low voltage electron microscope. The results indicated that a certain amount of (Fe,Cr)2O3 phases existed in the original ODS alloy. They did not change obviously after hydrogen ion implantation at room temperature. During heating the specimen implanted with hydrogen ions, however, the (Fe,Cr)2O3 phase dissolved gradually and the composition of the residual (Fe,Cr)2O3 phase changed too. On the contrary, the microstructure of the specimen which was not implanted with hydrogen ions did not changed obviously during heating, meanwhile, (Fe,Cr)2O3 phase did not dissolve.

     

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