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鎂合金AZ31動態再結晶行為的取向成像分析

Analysis on behavior of dynamic recrystallization in magnesium alloy AZ31 by orientation mapping

  • 摘要: 利用背散射電子衍射(EBSD)取向成像技術分析了具有不同初始織構的鎂合金AZ31動態再結晶晶粒的取向特征以及與相鄰的形變晶粒的取向關系.結果表明:不同初始織構以及不同應變量下動態再結晶新晶粒與形變晶粒的取向都相近,說明動態再結晶以連續方式進行,即亞晶轉動方式.隨形變量的增加,不同初始織構試樣的晶粒都轉向基面取向,但菊池帶襯度圖像顯示大的形變晶粒內部很少有亞晶界存在并且菊池帶質量高,說明塑性滑移機制仍在起很大作用但在靠近晶界處發生,形變晶粒是通過平行于壓縮面方向剪切晶界而逐漸消失的.動態再結晶晶粒與相鄰形變晶粒的取向差表明不同初始織構造成不同的取向差,但總的趨勢是相同的.

     

    Abstract: Orientation mapping based on EBSD technique is applied to reveal the orientation features of dynamic recrystallized grains and their neighboring matrix in a magnesium alloy AZ31 with different initial textures. The results show that, irrespective of initial texture and strain amount, new grains are similarly orientated to their neighboring matrix, illustrating a dynamic recrystallization through progressive subgrain rotation. In addition, the new grains gradually rotate to basal orientation in different samples, which indicates an important role of plastic slip during dynamic recrystallization in stead of superplastic deformation. The less subgrain boundaries in deformed grains under heavy strain were observed and these deformed grains have high quality of Kikuchi bands, which indicates that the deformed grains are consumed by the shear stress of grain boundaries parallel to the compression plane, rather than non-basal slip. The misorientation between the new and the deformed grains are measured and discussed in terms of the influence of initial texture.

     

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