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原位顆粒含量對半固態7075鋁合金組織的影響

Effect of the Volume Fraction of In-Situ TiC Particles on the Semi-Solid Micro-structure of Spray Formed 7075 Al Alloy

  • 摘要: 制備具有不同原位Tic顆粒含量的噴射沉積7075鋁合金,在610 ℃和620 ℃進行二次加熱并保溫30min,淬火固定半固態組織.采用掃描電鏡觀察其組織,利用平均截線法統計其晶粒尺寸,分析不同顆粒含量對噴射沉積7075鋁合金半固態組織的影響規律.結果表明:當TiC顆粒含量達到2.91%(體積分數)時已經產生良好的釘扎效果,使得合金基本保持噴射沉積組織特征,能夠滿足后續的半固態成形工藝要求;TiC顆粒含量超過2.91%后,晶粒尺寸會進一步減小,但晶界上的顆粒明顯增多并呈網狀分布;TiC顆粒含量小于2.91%時,局部區域發生晶粒的異常長大現象,使合金組織的均勻化程度下降.

     

    Abstract: The microstructure of in-situ reactive spray formed 7075+XTiC (the volume fraction X=0,1.15%, 1.73%, 2.91%, 4.48%, 5.95%) after heat treatment at 610℃ and 620℃ for 30min were observed using SEM. The grain size was measured by a mean linear intercept method to analyze the effect of different volume fractions of in-situ TiC particles on the semi-solid microstrucrure of spray formed 7075 alloy. It was shown that at 610℃ the pinning effect was significant when the volume fraction of in-situ TiC particles was up to 2.91%, which made micro-structures of the alloy keep as-spray formed characteristics and could meet the requirement of subsequent semi-solid processing. If that of in-situ TiC particles exceeded 2.91%, the grain size was further decreased, but the number of dispersoids and particles at grain boundaries evidently increased with net-shaped distribution. When that was less than 2.91%, the grain grew abnormally at local areas, resulting in the homogenization reduction of grain structure.

     

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