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Ce-TZP陶瓷材料中裂紋擴展路經的TEM觀察

TEM Observation of Crack Propagating Path in A Ce-TZP Ceramics

  • 摘要: 在透射電鏡(TEM)下原位觀察了,Ce-TZP陶瓷材料中裂紋擴展過程,發現其與一些金屬中裂紋擴展過程較相似,先在主裂紋前端形核微裂紋、微裂紋長大、然后主裂紋與微裂紋連接向前擴展。在裂尖應力場的作用下,裂尖附近有部分四方相發生馬氏體相變,增加了材料的斷裂韌性。同時還觀察到裂紋彎曲和轉向。實驗還發現在該材料中主裂紋尖端并不尖銳,而為鈍裂紋。

     

    Abstract: Crack propagating process in a Ce-TZP ceramics was in-situ observeed in TEM. It was found that the crack propagating process in this ceramics, similar to that in some metal materials, was microcrack nucleation ahead of main crack tip, microcrack growth, then main crack connecting with the micro one and propagating forward. The martensitic transformation of zirconia, induced by crack tip stress field, was observed in the vicinity of crack. Crack deflection was also observed in the ceramics. It was also found that the main crack tip was not sharp, it was a blunted crack.

     

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